สารบัญ

Contents
MENU

APPENDIX 1 GENERAL INFORMATION 1.1 Reagents


1.1 Reagents

                            APPENDIX 1 GENERAL INFORMATION
      The specifications given below are strictly for the use of the materials as reagents. The
inclusion of a material in this Appendix does not imply that it is suitable for use in medicines.
For materials or reagents whose availability is limited, a trademark or supplier’s name may
be indicated. It is however acceptable to use reagents from another source provided that
they comply with the standards of the Pharmacopoeia.
                                                 1.1 REAGENTS
        The name of a substance or solution indicates a reagent included in the following list.
The specifications given for reagents do not necessarily guarantee their quality for the
medicine.
        Some of the reagents included may be injurious to health. Important cautions have been
stated for these reagents. They should be handled in accordance with good laboratory
practice and any relevant regulations.
         Reagents in aqueous solution are prepared using water. Where the name of the solvent is
not stated, an aqueous solution is intended.
         Unless otherwise specified, the reagents and reagent solutions are to be stored in
well-closed containers. The labelling should comply with the relevant national legislation.
Ammonium Formate CH5NO2 = 63.06
Use analytical reagent grade of commerce.
DESCRIPTION Colourless, deliquescent crystals.
SOLUBILITY Soluble in water and in ethanol.
MELTING TEMPERATURE 116° (Appendix 4.3).
WEIGHT PER MILLILITRE 1.27 g (Appendix 4.9).

Store in tightly closed containers in a dry place.
Bisdemethoxycurcumin C19H16O4 = 308.33
Use analytical reagent grade of commerce containing not less than 98.0 per cent.
MELTING TEMPERATURE 224° (Appendix 4.3).

Store in tightly closed containers in a dry place at a temperature between 2° and 8°.
Reserpine C33H40N2O9 = 608.68
Use analytical reagent grade of commerce.
DESCRIPTION Creamy white to slightly yellow crystals or crystalline powder.
SOLUBILITY Very sparingly soluble in water; freely soluble in chloroform; soluble in benzene;
slightly soluble in acetone and in methanol.
MELTING RANGE 264° to 265°, with decomposition (Appendix 4.3).
SPECIFIC ROTATION About -118° at 23°, determined in chloroform (Appendix 4.5).

Store in tightly closed containers, protected from light, in a dry place at a temperature between 2° and 8°.

Ajmalicine C21H24N2O3 = 352.42
Use analytical reagent grade of commerce.
DESCRIPTION Beige powder.
SOLUBILITY Soluble in ethanol and in methanol.
MELTING TEMPERATURE 258° (Appendix 4.3).

Store in tightly closed containers in a dry place at a temperature between 2° and 8°.
Sennoside A C42H38O20 = 862.72
Use analytical reagent grade of commerce.
DESCRIPTION Rectangular yellow plates.
SOLUBILITY Insoluble in water; sparingly soluble in methanol.
MELTING RANGE 200° to 240°, with decomposition (Appendix 4.3).

Store in tightly closed containers in a dry place at a temperature between 2° and 8°.
Sennoside B C42H38O20 = 862.70
Use analytical reagent grade of commerce.
DESCRIPTION Light yellow prisms or fine needles.
SOLUBILITY Insoluble in water; sparingly soluble in methanol.
MELTING RANGE 180° to 186°, with decomposition (Appendix 4.3).

Store in tightly closed containers in a dry place at a temperature between 2° and 8°.
Puerarin C21H20O9 = 416.40
Use analytical reagent grade of commerce containing not less the 98.0 per cent.
DESCRIPTION White powder.

Store in tightly closed containers in a dry place at a temperature between 2° and 8°.
Daidzein C15H10O4 = 254.24
Use analytical reagent grade of commerce.
DESCRIPTION Pale yellow prisms.
SOLUBILITY Soluble in ethanol and in ether.
MELTING RANGE 315° to 323°, with decomposition (Appendix 4.3).

Store in tightly closed containers in a dry place at a temperature between 2° and 8°.
Formononetin C16H12O4 = 268.26
Use analytical reagent grade of commerce.
DESCRIPTION Needles.
MELTING TEMPERATURE About 258° (Appendix 4.3).

Store in tightly closed containers in a dry place at a temperature between 2° and 8°.

THP 2021 Supplement 2024 • APPENDIX 1 GENERAL INFORMATION 1.1 Reagents
view 279 ผู้เข้าชม / View
หมายเหตุ / Note :